2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol

Base Information

Chemical Name:2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol
CAS No.:479685-82-0
Molecular Formula:C₂₄H₄₀O₄
Molecular Weight:392.579
Hs Code.:

Synonyms:2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol

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Chemical Property of 2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol

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Technology Process of 2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol

There total 8 articles about 2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 479685-81-9
2-(n-undecyl)-6-benzyloxy-1-benzoyloxy-2-hexanol

: 479685-82-0
2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 4h; under 760 Torr;
DOI:10.1081/SCC-120005428

Reference yield:

: 111-29-5
1 ,5-pentanediol

: 479685-82-0
2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol

Guidance literature:: Multi-step reaction with 8 steps

1.1: 50 percent / sodium hydroxide / dimethylsulfoxide / 6 h / 20 °C

2.1: 73 percent / pyridinium chlorochromate / CH₂Cl₂ / 1 h / 20 °C

3.1: 66 percent / diethyl ether / 1.5 h / 0 - 20 °C

4.1: 71 percent / pyridinium dichromate / CH₂Cl₂ / 24 h / 20 °C

5.1: potassium tert-butoxide / tetrahydrofuran / 0.5 h / 0 °C

5.2: 99 percent / tetrahydrofuran / 0.5 h / 0 °C

6.1: 79 percent / 4-methylmorpholine N-oxide; osmium(VIII) oxide / 2-methyl-propan-2-ol; H₂O; acetone / 9 h / 20 °C

7.1: 97 percent / pyridine / CH₂Cl₂ / -60 - 20 °C

8.1: 86 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 4 h / 20 °C / 760 Torr

With pyridine; sodium hydroxide; osmium(VIII) oxide; dipyridinium dichromate; potassium tert-butylate; hydrogen; 4-methylmorpholine N-oxide; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetone; tert-butyl alcohol;
DOI:10.1081/SCC-120005428

Reference yield:

: 4541-15-5
5-(benzyloxy)-1-pentanol

: 479685-82-0
2-(n-undecyl)-1-benzoyloxy-2,6-hexanediol

Guidance literature:: Multi-step reaction with 7 steps

1.1: 73 percent / pyridinium chlorochromate / CH₂Cl₂ / 1 h / 20 °C

2.1: 66 percent / diethyl ether / 1.5 h / 0 - 20 °C

3.1: 71 percent / pyridinium dichromate / CH₂Cl₂ / 24 h / 20 °C

4.1: potassium tert-butoxide / tetrahydrofuran / 0.5 h / 0 °C

4.2: 99 percent / tetrahydrofuran / 0.5 h / 0 °C

5.1: 79 percent / 4-methylmorpholine N-oxide; osmium(VIII) oxide / 2-methyl-propan-2-ol; H₂O; acetone / 9 h / 20 °C

6.1: 97 percent / pyridine / CH₂Cl₂ / -60 - 20 °C

7.1: 86 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 4 h / 20 °C / 760 Torr

With pyridine; osmium(VIII) oxide; dipyridinium dichromate; potassium tert-butylate; hydrogen; 4-methylmorpholine N-oxide; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; water; ethyl acetate; acetone; tert-butyl alcohol;
DOI:10.1081/SCC-120005428