2-amino-3-azido-5,6-diphenylpyrazine

Base Information

Chemical Name:2-amino-3-azido-5,6-diphenylpyrazine
CAS No.:159755-92-7
Molecular Formula:C₁₆H₁₂N₆
Molecular Weight:288.311
Hs Code.:

Synonyms:2-amino-3-azido-5,6-diphenylpyrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-3-azido-5,6-diphenylpyrazine

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-amino-3-azido-5,6-diphenylpyrazine

There total 2 articles about 2-amino-3-azido-5,6-diphenylpyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 129108-83-4
2,3-diazido-5,6-diphenylpyrazine

: 64163-37-7
5,6-diphenyl-pyrazine-2,3-diamine

: 159755-92-7
2-amino-3-azido-5,6-diphenylpyrazine

Guidance literature:: With ammonium hydroxide; hydrogen; palladium on activated charcoal; In 1,2-dimethoxyethane; for 3h; Ambient temperature; Parr hydrogenation apparatus;
DOI:10.1055/s-1994-25607

Reference yield:

: 3-azido-2-chloro-5,6-diphenylpyrazine

: 159755-92-7
2-amino-3-azido-5,6-diphenylpyrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 97 percent sodium azide / dimethylformamide / 2.5 h / 80 °C

2: 58 percent / 28-30 percent ammonium hydroxide, H₂ / 10 percent Pd/C / 1,2-dimethoxy-ethane / 3 h / Ambient temperature; Parr hydrogenation apparatus

With ammonium hydroxide; sodium azide; hydrogen; palladium on activated charcoal; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1994-25607