2,3-bis(4-(trifluoromethyl)phenyl)fumaronitrile

Base Information

Chemical Name:2,3-bis(4-(trifluoromethyl)phenyl)fumaronitrile
CAS No.:521292-77-3
Molecular Formula:C₁₈H₈F₆N₂
Molecular Weight:366.265
Hs Code.:

Synonyms:2,3-bis(4-(trifluoromethyl)phenyl)fumaronitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-bis(4-(trifluoromethyl)phenyl)fumaronitrile

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Technology Process of 2,3-bis(4-(trifluoromethyl)phenyl)fumaronitrile

There total 1 articles about 2,3-bis(4-(trifluoromethyl)phenyl)fumaronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 2338-75-2
4-(Trifluoromethyl)phenylacetonitrile

: 521292-77-3
2,3-bis(4-(trifluoromethyl)phenyl)fumaronitrile

Guidance literature:: With iodine; sodium; In methanol; diethyl ether; at 20 ℃; Cooling with ice; Inert atmosphere;
DOI:10.1016/j.dyepig.2019.107829

Reference yield: 30.0%

: 521292-77-3
2,3-bis(4-(trifluoromethyl)phenyl)fumaronitrile

: 10025-82-8
indium(III) chloride

: (octakis(p-(trifluoromethyl)phenyl)tetraazaporphyrinato)indium(III) chloride

Guidance literature:: With catalyst: 1,8-diazabicyclo[5.4.0]undec-7-ene; In quinoline; the mixt. in quinoline in the presence of 5 drops of DBU was heated at 230°C for 8 h, slow cooled; CH3OH was added, stirred for 10 min, H2O was added, ppt. was centrifuged, CH3OH was removed, washing was repeated twice, to CH2Cl2-soln. methanol was added, evapd., ppt. was dried at 0.1 bar and 90°C, chromy. on silica gel (CH2Cl); elem. anal.;
DOI:10.1021/ic0205738