Technology Process of C28H23F3OSe
There total 4 articles about C28H23F3OSe which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
1.2: 0.17 h / -78 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 25 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C
3.2: 0.5 h / -78 - 25 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 25 °C
With
1H-imidazole; tetrabutyl ammonium fluoride; isopropylmagnesium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C
1.2: 0.5 h / -78 - 25 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 25 °C
With
tetrabutyl ammonium fluoride; lithium diisopropyl amide;
In
tetrahydrofuran;