2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside

Base Information

Chemical Name:2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside
CAS No.:861821-39-8
Molecular Formula:C₄₀H₄₈O₁₂
Molecular Weight:720.814
Hs Code.:

Synonyms:2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside

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Chemical Property of 2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside

There total 4 articles about 2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.3%

: 421558-11-4
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

: 115375-24-1
(E)-3-(4-(allyloxy)-3-methoxyphenyl)acrylic acid

: 861821-39-8
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 16h;
DOI:10.1016/j.carres.2005.04.011

Reference yield:

: 2-(4-allyloxyphenyl)ethyl 4,6-O-benzylidene-β-D-glucopyranoside

: 861821-39-8
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / dimethylformamide / 0.67 h

1.2: 81.4 percent / dimethylformamide / 10 h

2.1: 74.1 percent / aq. AcOH / 4 h / 80 °C

3.1: 92.2 percent / triethylamine / CH₂Cl₂ / 3 h

4.1: 92.3 percent / DCC; DMAP; 4A MS / CH₂Cl₂ / 16 h

With dmap; sodium hydride; acetic acid; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2005.04.011

Reference yield:

: 421558-10-3
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-β-D-glucopyranoside

: 861821-39-8
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4-O-[(E)-(4-O-allyl)feruloyl]-6-O-allyloxycarbonyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92.2 percent / triethylamine / CH₂Cl₂ / 3 h

2: 92.3 percent / DCC; DMAP; 4A MS / CH₂Cl₂ / 16 h

With dmap; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.carres.2005.04.011