2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside

Base Information

Chemical Name:2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside
CAS No.:421558-09-0
Molecular Formula:C₃₀H₃₆O₇
Molecular Weight:508.612
Hs Code.:

Synonyms:2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside

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Chemical Property of 2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside

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Technology Process of 2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside

There total 1 articles about 2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.4%

: 2-(4-allyloxyphenyl)ethyl 4,6-O-benzylidene-β-D-glucopyranoside

: 106-95-6
allyl bromide

: 421558-09-0
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: 2-(4-allyloxyphenyl)ethyl 4,6-O-benzylidene-β-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; for 0.666667h;

allyl bromide; In N,N-dimethyl-formamide; for 10h;
DOI:10.1016/j.carres.2005.04.011

Reference yield: 74.1%

: 421558-09-0
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside

: 421558-10-3
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-β-D-glucopyranoside

Guidance literature:: With acetic acid; at 80 ℃; for 4h;
DOI:10.1016/j.carres.2005.04.011

Reference yield:

: 421558-09-0
2-(4-allyloxyphenyl)ethyl 2,3-di-O-allyl-4,6-O-benzylidene-β-D-glucopyranoside

: 110344-59-7
2-(4-hydroxyphenyl)ethyl 4-Ο-(E)-Feruloyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 74.1 percent / aq. AcOH / 4 h / 80 °C

2: 92.2 percent / triethylamine / CH₂Cl₂ / 3 h

3: 92.3 percent / DCC; DMAP; 4A MS / CH₂Cl₂ / 16 h

4: 79.8 percent / p-TsOH / Pd/C / methanol; H₂O / 24 h / 60 - 80 °C

With dmap; toluene-4-sulfonic acid; acetic acid; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; water;
DOI:10.1016/j.carres.2005.04.011