N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine

Base Information

Chemical Name:N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine
CAS No.:825633-51-0
Molecular Formula:C₂₂H₂₉NO₂
Molecular Weight:339.478
Hs Code.:

Synonyms:N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine

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Technology Process of N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine

There total 1 articles about N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-46-9
benzylamine

: 188255-40-5
3-isopropoxy-4-methoxy-2-(1-methyl-2-propenyl)benzaldehyde

: 825633-51-0
N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine

Guidance literature:: benzylamine; 3-isopropoxy-4-methoxy-2-(1-methyl-2-propenyl)benzaldehyde; With toluene-4-sulfonic acid; In toluene; for 18h; Heating;

With sodium tetrahydroborate; water; In methanol; at 0 ℃; for 1h;
DOI:10.1016/j.tetlet.2004.10.155

Reference yield:

: 825633-51-0
N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine

: (+/-)-2-benzyl-5-isopropoxy-6-methoxy-3,4-cis-dimethyl-1,2,3,4-tetrahydroisoquinoline

: (+/-)-2-benzyl-5-isopropoxy-6-methoxy-3,4-trans-dimethyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: N-{[3-isopropoxy-4-methoxy-2-(1-methylprop-2-en-1-yl)phenyl]methyl}benzylamine; With mercury(II) diacetate; In tetrahydrofuran; water; at 20 ℃; for 24h;

With sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; water; at 20 ℃; for 24h; Further stages. Title compound not separated from byproducts.;
DOI:10.1002/ejoc.200700580