Technology Process of C44H46N2P4
There total 4 articles about C44H46N2P4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride; chloro-trimethyl-silane / tetrahydrofuran / 21 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
1.2: Inert atmosphere; Schlenk technique; Cooling with ice
2.1: acetonitrile / 65 °C / Inert atmosphere; Schlenk technique
3.1: ethanol / 65 °C / Inert atmosphere; Schlenk technique
With
lithium aluminium tetrahydride; chloro-trimethyl-silane;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/ic401232g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 2,2'-azobis(isobutyronitrile) / 21 h / 65 °C / Inert atmosphere; Schlenk technique
2.1: lithium aluminium tetrahydride; chloro-trimethyl-silane / tetrahydrofuran / 21 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
2.2: Inert atmosphere; Schlenk technique; Cooling with ice
3.1: acetonitrile / 65 °C / Inert atmosphere; Schlenk technique
4.1: ethanol / 65 °C / Inert atmosphere; Schlenk technique
With
lithium aluminium tetrahydride; chloro-trimethyl-silane; 2,2'-azobis(isobutyronitrile);
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/ic401232g