diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate

Base Information

Chemical Name:diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate
CAS No.:1260074-30-3
Molecular Formula:C₄₄H₅₄N₈O₄
Molecular Weight:758.964
Hs Code.:

Synonyms:diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate

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Chemical Property of diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate

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Technology Process of diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate

There total 3 articles about diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1260074-31-4
N₁,N₁'-(1,3-phenylenebis(methylene))bis(N₂,N₂'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine)

: 105-36-2
ethyl bromoacetate

: 1260074-30-3
diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c0dt00165a

Reference yield:

: 189440-33-3
(2-aminoethyl)bis(2-pyridylmethyl)amine

: 1260074-30-3
diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 24 h / Molecular sieve; Inert atmosphere; Reflux

2: sodium tetrahydroborate / methanol / 3 h / Molecular sieve; Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;
DOI:10.1039/c0dt00165a

Reference yield:

: 626-19-7
Isophthalaldehyde

: 1260074-30-3
diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 24 h / Molecular sieve; Inert atmosphere; Reflux

2: sodium tetrahydroborate / methanol / 3 h / Molecular sieve; Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;
DOI:10.1039/c0dt00165a