trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3

Base Information

• Chemical Name: trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3
• CAS No.: 96841-82-6
• Molecular Formula: CF₃O₃S*C₁₄H₂₀NO
• Molecular Weight: 367.389

Synonyms:trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3

Chemical Property of trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3

Chemical Property:

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Technology Process of trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3

There total 2 articles about trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

mesitylene-2-carboxylic acid chloride (938-18-1) → trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3 (96841-82-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / Et₃N / benzene / 24 h / Heating

2: CH₂Cl₂

With triethylamine; In dichloromethane; benzene;

DOI:10.1016/S0040-4020(01)91331-6

Reference yield:

2-mesityl-5,6-dihydro oxazine (96841-76-8) + methyl trifluoromethanesulfonate (333-27-7) → trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3 (96841-82-6)

Guidance literature:

In dichloromethane;

DOI:10.1016/S0040-4020(01)91331-6

Reference yield: 95.0%

trifluoromethane sulfonates de N-methyl(trimethyl-2,4,6 phenyl)-2 dihydro-5,6 oxazinium-1,3 (96841-82-6) → C18H29NO

Guidance literature:

In diethyl ether; at 0 ℃; for 2h;

DOI:10.1016/S0040-4039(00)98499-5

upstream raw materials:

2-mesityl-5,6-dihydro oxazine

methyl trifluoromethanesulfonate

mesitylene-2-carboxylic acid chloride

Downstream raw materials:

N-methyl,N-(4-cyano,4-carboethoxybutyl)mesityl amide

N-methyl,N-(4,4-dicarboethoxybutyl)mesityl amide

N-methyl, N-(4,4-diphenylsulfonebutyl)mesityl amide

N-Butyl-2,4,6,N-tetramethyl-benzamide

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