Technology Process of C11H12O5
There total 5 articles about C11H12O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethyl acetate;
at 20 ℃;
for 0.5h;
under 760.051 Torr;
chemoselective reaction;
DOI:10.1016/j.tetlet.2011.07.063
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 40 ℃;
for 24h;
chemoselective reaction;
DOI:10.1016/j.tetlet.2011.07.063
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / 70 °C
2: triethylamine; magnesium chloride / 80 °C
3: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 60 °C
4: diphenyl diselenide; dihydrogen peroxide / dichloromethane / 48 h / 20 °C
5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 0.5 h / 20 °C / 760.05 Torr
With
diphenyl diselenide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; potassium carbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; magnesium chloride;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
4: Baeyer-Villiger oxidation;
DOI:10.1016/j.tetlet.2011.07.063