tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate

Base Information

Chemical Name:tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate
CAS No.:1338684-74-4
Molecular Formula:C₂₆H₂₉N₅O₄
Molecular Weight:475.547
Hs Code.:

Synonyms:tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate

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Chemical Property of tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate

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Technology Process of tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate

There total 4 articles about tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338684-73-3
tert-butyl (1-((2-amino-4,5-dimethylphenyl)amino)-3-phenylpropan-2-yl)carbamate

: 2244-11-3
alloxan monohydrate

: 1338684-74-4
tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate

Guidance literature:: With boric acid; acetic acid; at 20 ℃; for 1.5h;

Reference yield:

: 6972-71-0
4,5-dimethyl-2-nitrobenzenamine

: 1338684-74-4
tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide / water / 0.5 h / 70 °C

1.2: 0.25 h / -5 °C

1.3: 0 - 70 °C

2.1: dimethyl sulfoxide / 1 h / 130 °C

3.1: sodium tetrahydroborate; methanol / palladium 10% on activated carbon / ethyl acetate / 0.33 h / 20 °C / Inert atmosphere

4.1: boric acid; acetic acid / 1.5 h / 20 °C

With methanol; sodium tetrahydroborate; hydrogen bromide; boric acid; acetic acid; palladium 10% on activated carbon; In water; dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 53938-24-2
1-bromo-4,5-dimethyl-2-nitrobenzene

: 1338684-74-4
tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 1 h / 130 °C

2: sodium tetrahydroborate; methanol / palladium 10% on activated carbon / ethyl acetate / 0.33 h / 20 °C / Inert atmosphere

3: boric acid; acetic acid / 1.5 h / 20 °C

With methanol; sodium tetrahydroborate; boric acid; acetic acid; palladium 10% on activated carbon; In dimethyl sulfoxide; ethyl acetate;