10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Base Information

Chemical Name:10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione
CAS No.:1338684-71-1
Molecular Formula:C₂₁H₂₁N₅O₂
Molecular Weight:375.43
Hs Code.:

Synonyms:10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

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Technology Process of 10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

There total 6 articles about 10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1338684-74-4
tert-butyl (1-(7,8-dimethyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)-3-phenylpropan-2-yl)carbamate

: 1338684-71-1
10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.75h;

Reference yield:

: 6972-71-0
4,5-dimethyl-2-nitrobenzenamine

: 1338684-71-1
10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen bromide / water / 0.5 h / 70 °C

1.2: 0.25 h / -5 °C

1.3: 0 - 70 °C

2.1: dimethyl sulfoxide / 1 h / 130 °C

3.1: sodium tetrahydroborate; methanol / palladium 10% on activated carbon / ethyl acetate / 0.33 h / 20 °C / Inert atmosphere

4.1: boric acid; acetic acid / 1.5 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

With methanol; sodium tetrahydroborate; hydrogen bromide; boric acid; acetic acid; trifluoroacetic acid; palladium 10% on activated carbon; In dichloromethane; water; dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 53938-24-2
1-bromo-4,5-dimethyl-2-nitrobenzene

: 1338684-71-1
10-(2-amino-3-phenylpropyl)-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 4 steps

1: dimethyl sulfoxide / 1 h / 130 °C

2: sodium tetrahydroborate; methanol / palladium 10% on activated carbon / ethyl acetate / 0.33 h / 20 °C / Inert atmosphere

3: boric acid; acetic acid / 1.5 h / 20 °C

4: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

With methanol; sodium tetrahydroborate; boric acid; acetic acid; trifluoroacetic acid; palladium 10% on activated carbon; In dichloromethane; dimethyl sulfoxide; ethyl acetate;