3-(4-methoxyphenyl)-3-methylpent-4-enal

Base Information

Chemical Name:3-(4-methoxyphenyl)-3-methylpent-4-enal
CAS No.:174229-47-1
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:3-(4-methoxyphenyl)-3-methylpent-4-enal

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Chemical Property of 3-(4-methoxyphenyl)-3-methylpent-4-enal

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Technology Process of 3-(4-methoxyphenyl)-3-methylpent-4-enal

There total 3 articles about 3-(4-methoxyphenyl)-3-methylpent-4-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 862982-44-3
ethyl 3-(4-methoxyphenyl)-3-methylpent-4-enoate

: 174229-47-1
3-(4-methoxyphenyl)-3-methylpent-4-enal

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / lithium aluminium hydride / diethyl ether / 1 h / 0 °C

2: 88 percent / pyridinium chlorochromate; silica gel / CH₂Cl₂ / 0.5 h / 20 °C

With lithium aluminium tetrahydride; silica gel; pyridinium chlorochromate; In diethyl ether; dichloromethane;
DOI:10.1081/SCC-200061679

Reference yield:

: 108454-55-3,122669-85-6,7706-82-3
3-(4-methoxyphenyl)-2-butenoic acid ethyl ester

: 174229-47-1
3-(4-methoxyphenyl)-3-methylpent-4-enal

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / lithium aluminium hydride / diethyl ether / 1 h / -90 - -20 °C

2: 69 percent / propionic acid / 48 h / 180 °C

3: 92 percent / lithium aluminium hydride / diethyl ether / 1 h / 0 °C

4: 88 percent / pyridinium chlorochromate; silica gel / CH₂Cl₂ / 0.5 h / 20 °C

With lithium aluminium tetrahydride; silica gel; propionic acid; pyridinium chlorochromate; In diethyl ether; dichloromethane; 2: Claisen rearrangement;
DOI:10.1081/SCC-200061679

Reference yield:

: 132533-07-4
(E)-3-(4-methoxyphenyl)but-2-ene-1-ol

: 174229-47-1
3-(4-methoxyphenyl)-3-methylpent-4-enal

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / propionic acid / 48 h / 180 °C

2: 92 percent / lithium aluminium hydride / diethyl ether / 1 h / 0 °C

3: 88 percent / pyridinium chlorochromate; silica gel / CH₂Cl₂ / 0.5 h / 20 °C

With lithium aluminium tetrahydride; silica gel; propionic acid; pyridinium chlorochromate; In diethyl ether; dichloromethane; 1: Claisen rearrangement;
DOI:10.1081/SCC-200061679