4-[H-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OH

Base Information

Chemical Name:4-[H-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OH
CAS No.:1203698-17-2
Molecular Formula:C₃₉H₆₈N₈O₁₁SSi
Molecular Weight:885.167
Hs Code.:

Synonyms:4-[H-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[H-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OH

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Technology Process of 4-[H-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OH

There total 1 articles about 4-[H-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1203698-15-0
4-[Z-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OBn

: 1203698-17-2
4-[H-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OH

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃;
DOI:10.1039/b914836a

Reference yield: 66.0%

: 1203698-17-2
4-[H-Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp-Arg(Mtr)-Gly-OH

: cyclo[Arg(Mtr)-Gly-4-[Asp(Ot-Bu)]-1-(2-(tert-butyldimethylsilyloxy)ethyl)Amp]

Guidance literature:: With 2,4,6-trimethyl-pyridine; 1-hydroxy-7-aza-benzotriazole; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1039/b914836a