1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile

Base Information

Chemical Name:1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile
CAS No.:115592-34-2
Molecular Formula:C₂₄H₁₈N₄O₂
Molecular Weight:394.433
Hs Code.:

Synonyms:1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile

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Chemical Property of 1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile

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Technology Process of 1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile

There total 4 articles about 1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2700-22-3
Benzylidenemalononitrile

: 115592-31-9
6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile

: 115592-34-2
1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile

Guidance literature:: With piperidine; In ethanol; for 3h; Heating;

Reference yield:

: 115592-31-9
6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile

: 115592-34-2
1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1. Na / 1. dioxane, 5 min, reflux; 2. dioxane, 8 h, reflux

2: 1. Na / 1. dioxane, 5 min, reflux; 2. dioxane, 10 h, reflux

With sodium;

Reference yield:

: 24756-04-5
3-[(4-methylphenyl)hydrazono]pentane-2,4-dione

: 115592-34-2
1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / ammonium acetate / 0.5 h / 160 °C

2: 1. Na / 1. dioxane, 5 min, reflux; 2. dioxane, 8 h, reflux

3: 1. Na / 1. dioxane, 5 min, reflux; 2. dioxane, 10 h, reflux

With ammonium acetate; sodium;