6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile

Base Information

• Chemical Name: 6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile
• CAS No.: 115592-31-9
• Molecular Formula: C₁₅H₁₃N₃O₂
• Molecular Weight: 267.287

Synonyms:6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile

Chemical Property of 6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile

Chemical Property:

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Technology Process of 6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile

There total 1 articles about 6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

ethyl 2-cyanoacetate (105-56-6) + 3-[(4-methylphenyl)hydrazono]pentane-2,4-dione (24756-04-5) → 6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile (115592-31-9)

Guidance literature:

With ammonium acetate; at 160 ℃; for 0.5h;

Reference yield: 73.0%

furfural (98-01-1) + 6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile (115592-31-9) → 6-Acetyl-5-((E)-2-furan-2-yl-vinyl)-3-oxo-2-p-tolyl-2,3-dihydro-pyridazine-4-carbonitrile (125040-90-6)

Guidance literature:

With piperidine; In 1,4-dioxane; for 3h; Heating;

Reference yield: 70.0%

2-(4-methoxyphenylmethylene)malononitrile (2826-26-8) + 6-acetyl-2,3-dihydro-5-methyl-3-oxo-2-(p-tolyl)-4-pyridazinecarbonitrile (115592-31-9) → 1-Acetyl-5-amino-7-(4-methoxy-phenyl)-4-oxo-3-p-tolyl-3,4-dihydro-phthalazine-6-carbonitrile (125040-95-1)

Guidance literature:

With piperidine; In 1,4-dioxane; for 1h; Heating;

upstream raw materials:

ethyl 2-cyanoacetate

3-[(4-methylphenyl)hydrazono]pentane-2,4-dione

Downstream raw materials:

6-Acetyl-5-((E)-2-furan-2-yl-vinyl)-3-oxo-2-p-tolyl-2,3-dihydro-pyridazine-4-carbonitrile

1-Acetyl-5-amino-7-(4-methoxy-phenyl)-4-oxo-3-p-tolyl-3,4-dihydro-phthalazine-6-carbonitrile

1-acetyl-5-amino-3,4-dihydro-4-oxo-7-phenyl-3-(p-tolyl)-6-phthalazinecarbonitrile

1-Acetyl-5-amino-7-furan-2-yl-4-oxo-3-p-tolyl-3,4-dihydro-phthalazine-6-carbonitrile

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