1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone

Base Information

Chemical Name:1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone
CAS No.:119384-66-6
Molecular Formula:C₃₈H₃₂O₇
Molecular Weight:600.668
Hs Code.:

Synonyms:1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone

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Chemical Property of 1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone

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Technology Process of 1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone

There total 8 articles about 1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 124662-51-7
1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2-propen-1-one

: 119384-66-6
1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In 1,4-dioxane; methanol; for 3h; Ambient temperature;
DOI:10.1248/cpb.37.1441

Reference yield:

: 1835-11-6
4-benzyloxy-3-methoxyacetophenone

: 119384-66-6
1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / KOH / ethanol

2: 87 percent / conc. HCl / methanol; dioxane

3: 92 percent / 30percent H₂O₂, 5percent NaOH / methanol; dioxane

With hydrogenchloride; potassium hydroxide; sodium hydroxide; dihydrogen peroxide; In 1,4-dioxane; methanol; ethanol;
DOI:10.1039/c39880000749

Reference yield:

: 119384-63-3
5-bromo-3,4-benzyloxybenzaldehyde dimethyl acetal

: 119384-66-6
1-(4-benzyloxy-3-methoxyphenyl)-3-(2,3-dibenzyloxy-5-formylphenyl)-2,3-epoxy-1-propanone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) Et₂O, -78 deg C, 2.) -78 to r.t.

2: 93 percent / KOH / ethanol

3: 87 percent / conc. HCl / methanol; dioxane

4: 92 percent / 30percent H₂O₂, 5percent NaOH / methanol; dioxane

With hydrogenchloride; potassium hydroxide; sodium hydroxide; n-butyllithium; dihydrogen peroxide; In 1,4-dioxane; methanol; ethanol;
DOI:10.1039/c39880000749