C₁₅H₂₁NO₂S

Base Information

Chemical Name:C₁₅H₂₁NO₂S
CAS No.:1574474-98-8
Molecular Formula:C₁₅H₂₁NO₂S
Molecular Weight:279.403
Hs Code.:

C<sub>15</sub>H<sub>21</sub>NO<sub>2</sub>S

Synonyms:C₁₅H₂₁NO₂S

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Chemical Property of C₁₅H₂₁NO₂S

Chemical Property:

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Technology Process of C₁₅H₂₁NO₂S

There total 8 articles about C₁₅H₂₁NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 804553-24-0
2-(3-oxobutyl)benzaldehyde

: 1574474-98-8
C₁₅H₂₁NO₂S

Guidance literature:: With potassium hydrogensulfate; In toluene; at 20 ℃; for 18h;
DOI:10.1080/00397911.2013.841938

Reference yield:

: 86867-62-1,91388-37-3
(E)-3-(2-formylphenyl)propenoic acid ethyl ester

: 1574474-98-8
C₁₅H₂₁NO₂S

Guidance literature:: Multi-step reaction with 8 steps

1: toluene-4-sulfonic acid / methanol / Molecular sieve; Reflux

2: hydrogen; palladium 10% on activated carbon / methanol / 1.5 h / 35 °C

3: sodium hydroxide / methanol; tetrahydrofuran / 0.5 h / 20 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / 18 h / 20 °C

5: toluene-4-sulfonic acid / methanol / Molecular sieve; Reflux

6: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

7: hydrogenchloride / water / 0.25 h / 20 °C / Inert atmosphere

8: potassium hydrogensulfate / toluene / 18 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; dmap; potassium hydrogensulfate; n-butyllithium; palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1080/00397911.2013.841938

Reference yield:

: 1574475-06-1
C₁₄H₂₀O₄

: 1574474-98-8
C₁₅H₂₁NO₂S

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / methanol; tetrahydrofuran / 0.5 h / 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / 18 h / 20 °C

3: toluene-4-sulfonic acid / methanol / Molecular sieve; Reflux

4: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

5: hydrogenchloride / water / 0.25 h / 20 °C / Inert atmosphere

6: potassium hydrogensulfate / toluene / 18 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; dmap; potassium hydrogensulfate; n-butyllithium; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1080/00397911.2013.841938