Technology Process of C23H18N6
There total 3 articles about C23H18N6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammonium acetate; palladium diacetate;
In
1-methyl-pyrrolidin-2-one;
at 100 ℃;
for 22h;
DOI:10.1016/j.bmcl.2012.12.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(II) sulfate; sodium L-ascorbate; sodium hydrogencarbonate / N,N-dimethyl-formamide; water / 18 h / 20 - 100 °C
2: tetrabutylammonium acetate; palladium diacetate / 1-methyl-pyrrolidin-2-one / 22 h / 100 °C
With
sodium L-ascorbate; tetrabutylammonium acetate; palladium diacetate; sodium hydrogencarbonate; copper(II) sulfate;
In
1-methyl-pyrrolidin-2-one; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.12.008
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide / dimethyl sulfoxide / 20 h / 120 °C
2: copper(II) sulfate; sodium L-ascorbate; sodium hydrogencarbonate / N,N-dimethyl-formamide; water / 18 h / 20 - 100 °C
3: tetrabutylammonium acetate; palladium diacetate / 1-methyl-pyrrolidin-2-one / 22 h / 100 °C
With
sodium azide; sodium L-ascorbate; tetrabutylammonium acetate; palladium diacetate; sodium hydrogencarbonate; copper(II) sulfate;
In
1-methyl-pyrrolidin-2-one; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.12.008
