N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

Base Information

Chemical Name:N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside
CAS No.:128775-50-8
Molecular Formula:C₆₁H₆₁NO₁₇
Molecular Weight:1080.15
Hs Code.:

N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

Synonyms:N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

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Chemical Property of N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

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Technology Process of N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

There total 15 articles about N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 128801-20-7
N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-4-O-dichloroacetyl-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

: 128775-50-8
N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

Guidance literature:: With ammonium hydroxide; In methanol; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)89206-1

Reference yield:

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 128775-50-8
N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1: 74 percent / mercuric bromide, mercuric cyanide / acetonitrile / 4 h / Ambient temperature

2: 98 percent / NaOMe / methanol / 17 h / Ambient temperature

3: 79 percent / p-TsOH / acetone / 4 h / Ambient temperature

4: pyridine / 2 h / Ambient temperature

5: H₂O / acetic acid / 1 h / 50 °C

6: 85 percent / Et₃N / 1,2-dichloro-ethane / 17 h / Ambient temperature

7: 80 percent / silver trifluoromethanesulphonate, 1M methylsulphenyl bromide / 1,2-dichloro-ethane / 2 h / Ambient temperature

8: 82 percent / 25percent aq. ammonium hydroxide / methanol / 2 h / Ambient temperature

With pyridine; ammonium hydroxide; methylsulfenyl bromide; water; sodium methylate; silver trifluoromethanesulfonate; mercury(II) cyanide; toluene-4-sulfonic acid; triethylamine; mercury dibromide; In methanol; acetic acid; 1,2-dichloro-ethane; acetone; acetonitrile;
DOI:10.1016/S0040-4020(01)89206-1

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 128775-50-8
N-benzyloxycarbonyl-3-aminopropyl 2,3-di-O-benzoyl-4-O-<2,3-di-O-(2-methylbenzoyl)-α-L-rhamnopyranosyl>-6-O-(2-methylbenzoyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1: 74 percent / mercuric bromide, mercuric cyanide / acetonitrile / 4 h / Ambient temperature

2: 98 percent / NaOMe / methanol / 17 h / Ambient temperature

3: 79 percent / p-TsOH / acetone / 4 h / Ambient temperature

4: pyridine / 2 h / Ambient temperature

5: H₂O / acetic acid / 1 h / 50 °C

6: 85 percent / Et₃N / 1,2-dichloro-ethane / 17 h / Ambient temperature

7: 80 percent / silver trifluoromethanesulphonate, 1M methylsulphenyl bromide / 1,2-dichloro-ethane / 2 h / Ambient temperature

8: 82 percent / 25percent aq. ammonium hydroxide / methanol / 2 h / Ambient temperature

With pyridine; ammonium hydroxide; methylsulfenyl bromide; water; sodium methylate; silver trifluoromethanesulfonate; mercury(II) cyanide; toluene-4-sulfonic acid; triethylamine; mercury dibromide; In methanol; acetic acid; 1,2-dichloro-ethane; acetone; acetonitrile;
DOI:10.1016/S0040-4020(01)89206-1