(2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one

Base Information

• Chemical Name: (2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one
• CAS No.: 353449-35-1
• Molecular Formula: C₃₀H₄₁NO₄Si
• Molecular Weight: 507.745

Synonyms:(2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one

Chemical Property of (2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one

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Technology Process of (2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one

There total 1 articles about (2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-[2-(tert-butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-2-methyl-2,6,7,8-tetrahydro-1H-quinolin-5-one → (2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one (353449-35-1)

Guidance literature:

With osmium(VIII) oxide; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; for 24h; Heating;

DOI:10.1021/ol010034r

Reference yield: 90.0%

(2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one (353449-35-1) → C30H39NO3Si (1196903-30-6)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; at 80 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1055/s-0029-1216920

Reference yield: 80.0%

(2S,3S,4R)-1-[(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1,2-diphenyl-ethyl]-3,4-dihydroxy-2-methyl-2,3,4,6,7,8-hexahydro-1H-quinolin-5-one (353449-35-1) → C30H41NO3Si (1072157-48-2)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at -20 - -10 ℃; Inert atmosphere;

DOI:10.1021/ol802068q

Downstream raw materials:

C₃₀H₄₁NO₃Si

C₃₀H₃₉NO₃Si

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