(2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid

Base Information

Chemical Name:(2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid
CAS No.:175844-87-8
Molecular Formula:C₄₀H₄₁O₉P
Molecular Weight:696.734
Hs Code.:

Synonyms:(2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid

Chemical Property:

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Technology Process of (2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid

There total 4 articles about (2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 175844-86-7
Phosphoric acid dibenzyl ester (2R,3R,4S)-2,3,4-tris-benzyloxy-5-oxo-pentyl ester

: 175844-87-8
(2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide; Yield given;
DOI:10.1016/0040-4039(96)00004-4

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 175844-87-8
(2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent

2: HgCl₂, CaCO₃ / acetonitrile; H₂O

3: PDC / dimethylformamide

With dipyridinium dichromate; calcium carbonate; mercury dichloride; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0040-4039(96)00004-4

Reference yield:

: 108713-91-3
2,3,4-tri-O-benzyl-D-arabinose diethyl dithioacetal

: 175844-87-8
(2S,3R,4R)-2,3,4-Tris-benzyloxy-5-(bis-benzyloxy-phosphoryloxy)-pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent

2: HgCl₂, CaCO₃ / acetonitrile; H₂O

3: PDC / dimethylformamide

With dipyridinium dichromate; calcium carbonate; mercury dichloride; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0040-4039(96)00004-4