tricarbonyl bis(tri-p-tolylphosphine) iron

Base Information

Chemical Name:tricarbonyl bis(tri-p-tolylphosphine) iron
CAS No.:52500-74-0
Molecular Formula:C₄₅H₄₂FeO₃P₂
Molecular Weight:748.621
Hs Code.:

Synonyms:tricarbonyl bis(tri-p-tolylphosphine) iron

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Chemical Property of tricarbonyl bis(tri-p-tolylphosphine) iron

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of tricarbonyl bis(tri-p-tolylphosphine) iron

There total 5 articles about tricarbonyl bis(tri-p-tolylphosphine) iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: K⁽¹⁺⁾*H⁽¹⁺⁾*Fe(CO)4^(2-)=KHFe(CO)4

: 1038-95-5,218281-19-7
Tri(p-tolyl)phosphine

: 52500-74-0
tricarbonyl bis(tri-p-tolylphosphine) iron

Guidance literature:: In ethanol; other Radiation; under N2; EtOH soln. of KHFe(CO)4 added to P(C6H5CH3)3; heated in microwave reactor (150 W, 5 min, 100°C, max T=112°C, max P=50 psi); cooled to room temp.; ppt. collected by suction filtration; washed with H2O and EtOH; dried;
DOI:10.1021/om900821c

Reference yield: 43.0%

: 15321-51-4
diiron nonacarbonyl

: 26516-62-1,52866-94-1
N-sulphinyl-p-bromoaniline

: 1038-95-5,218281-19-7
Tri(p-tolyl)phosphine

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 52500-74-0
tricarbonyl bis(tri-p-tolylphosphine) iron

: 52278-75-8,52553-46-5
(CO)4FeP(C₆H₄CH₃-p)3

: 85134-89-0
[Fe(P(4-MeC₆H₄)3)2(CO)2(4-BrC₆H₄NSO)]

Guidance literature:: In tetrahydrofuran; under N2, mixt. of Fe-complex, 4-BrC6H4NSO and (4-MeC6H4)3P (molar ratio 1:1:2) in THF were stirred for 1-4 h at room temp.; filtered, recrystd. from ether-MeOH or CH2Cl2-hexane; elem. anal.;

Reference yield: 40.0%

: 15321-51-4
diiron nonacarbonyl

: 13165-68-9,52867-11-5
4-ClC₆H₄NSO

: 1038-95-5,218281-19-7
Tri(p-tolyl)phosphine

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 52500-74-0
tricarbonyl bis(tri-p-tolylphosphine) iron

: 52278-75-8,52553-46-5
(CO)4FeP(C₆H₄CH₃-p)3

: 85134-88-9
[Fe(P(4-MeC₆H₄)3)2(CO)2(4-ClC₆H₄NSO)]

Guidance literature:: In tetrahydrofuran; under N2, mixt. of Fe-complex, 4-ClC6H4NSO and (4-MeC6H4)3P (molar ratio 1:1:2) in THF were stirred for 1-4 h at room temp.; filtered, recrystd. from ether-MeOH or CH2Cl2-hexane; elem. anal.;