3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole

Base Information

• Chemical Name: 3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole
• CAS No.: 1163299-96-4
• Molecular Formula: C₁₈H₁₁ClN₄OS
• Molecular Weight: 366.831

Synonyms:3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole

Chemical Property of 3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole

Chemical Property:

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Technology Process of 3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole

There total 1 articles about 3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2-amino-5-benzo[d]isoxazol-3-ylmethyl-[1,3,4]thiadiazole (1163299-94-2) + 4-chlorobenzoylmethyl bromide (536-38-9) → 3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole (1163299-96-4)

Guidance literature:

2-amino-5-benzo[d]isoxazol-3-ylmethyl-[1,3,4]thiadiazole; 4-chlorobenzoylmethyl bromide; In ethanol; for 18h; Reflux;

With sodium carbonate; In water;

DOI:10.1016/j.ejmech.2008.12.019

Reference yield: 75.0%

3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole (1163299-96-4) → 3-[5-bromo-6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole (1163300-02-4)

Guidance literature:

3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole; With bromine; sodium acetate; acetic acid; at 20 ℃;

With ammonia; In water;

DOI:10.1016/j.ejmech.2008.12.019

Reference yield: 35.0%

3-[6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole (1163299-96-4) → 3-[6-(4-chlorophenyl)-5-nitrosoimidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole (1163300-08-0)

Guidance literature:

With acetic acid; sodium nitrite; In water; at 20 ℃; Reflux;

DOI:10.1016/j.ejmech.2008.12.019

upstream raw materials:

2-amino-5-benzo[d]isoxazol-3-ylmethyl-[1,3,4]thiadiazole

4-chlorobenzoylmethyl bromide

Downstream raw materials:

3-[5-bromo-6-(4-chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole

3-[6-(4-chlorophenyl)-5-nitrosoimidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole

3-[6-(4-chlorophenyl)-5-thiocyanatoimidazo[2,1-b][1,3,4]thiadiazol-2-ylmethyl]benzo[d]isoxazole

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