4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester

Base Information

• Chemical Name: 4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester
• CAS No.: 39986-45-3
• Molecular Formula: C₁₅H₂₀ClN₃O₃
• Molecular Weight: 325.795

Synonyms:4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester

Chemical Property of 4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester

Chemical Property:

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Technology Process of 4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester

There total 2 articles about 4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroformic acid ethyl ester (541-41-3) + N-(4-Chloro-phenyl)-2-piperazin-1-yl-acetamide (54257-79-3) → 4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester (39986-45-3)

Guidance literature:

With sodium carbonate; In ethanol; at 20 ℃;

DOI:10.1002/ardp.200900117

Reference yield:

→ 4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester (39986-45-3)

Guidance literature:

2-Chloro-4'-chloroacetanilid, 1-Carbethoxypiperazin;

Reference yield: 59.0%

4-[(4-chloro-phenylcarbamoyl)-methyl]-piperazine-1-carboxylic acid ethyl ester (39986-45-3) → 4-(2-(4-chlorophenylamino)-2-oxoethyl)-N-hydroxypiperazine-1-carboxamide (1226513-53-6)

Guidance literature:

With hydroxylamine hydrochloride; In methanol; at 20 ℃;

DOI:10.1002/ardp.200900117

upstream raw materials:

chloroformic acid ethyl ester

N-(4-Chloro-phenyl)-2-piperazin-1-yl-acetamide

Downstream raw materials:

4-(2-(4-chlorophenylamino)-2-oxoethyl)-N-hydroxypiperazine-1-carboxamide

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