tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate

Base Information

Chemical Name:tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate
CAS No.:1333145-64-4
Molecular Formula:C₁₇H₂₁F₃N₄O₃
Molecular Weight:386.374
Hs Code.:

Synonyms:tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate

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Chemical Property of tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate

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Technology Process of tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate

There total 1 articles about tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 75178-96-0
N-Boc-1,3-diaminopropane

: 85559-46-2
4-[3-(trifluoromethyl)-3H-diazirin-3-yl]benzoic acid

: 1333145-64-4
tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate

Guidance literature:: 4-[3-(trifluoromethyl)-3H-diazirin-3-yl]benzoic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

N-Boc-1,3-diaminopropane; In dichloromethane; at 20 ℃; for 13h; Inert atmosphere;
DOI:10.1021/jm200692n

Reference yield: 87.0%

: 1333145-64-4
tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate

: 1333145-62-2
N-(3-aminopropyl)-4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamide

Guidance literature:: With hydrogenchloride; In methanol; water; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1021/jm200692n

Reference yield:

: 1333145-64-4
tert-butyl-3-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)benzamido)propylcarbamate

: C₆₅H₁₁₁F₃N₄O₁₀Si₃

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; water / 14 h / 20 °C / Inert atmosphere

2: triethylamine / methanol; dichloromethane / 120 h / 20 °C / Inert atmosphere

With hydrogenchloride; triethylamine; In methanol; dichloromethane; water;
DOI:10.1021/jm200692n