2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid

Base Information

Chemical Name:2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid
CAS No.:1374969-96-6
Molecular Formula:C₁₅H₉ClN₆O₂
Molecular Weight:340.728
Hs Code.:

Synonyms:2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid

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Chemical Property of 2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid

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Technology Process of 2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid

There total 1 articles about 2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 919354-52-2
ethyl 2,6-dichloro-5-cyanopyridine-3-carboxylate

: 626248-56-4
3-(2H-1,2,3-triazol-2-yl)aniline

: 1374969-96-6
2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid

Guidance literature:: ethyl 2,6-dichloro-5-cyanopyridine-3-carboxylate; 3-(2H-1,2,3-triazol-2-yl)aniline; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 15h;

With lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 2h; pH=2;

Reference yield:

: 1374969-96-6
2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid

: 2592-95-2
benzotriazol-1-ol

: 1374969-97-7
6-(1H-benzo[d][1,2,3]traizol-1-yloxy)-2-(3-(2H-1,2,3-trazol-2-yl)phenylamino)-5-cyanonicotinamide

Guidance literature:: 2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid; benzotriazol-1-ol; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

With ammonia; In 1,4-dioxane; for 0.166667h;

Reference yield:

: 1374969-96-6
2-(3-(2H)-1,2,3-triazol-2-yl)phenylamino-6-chloro-5-cyanonicotinic acid

: 1374970-09-8
2-(3-(2H-1,2,3-triazol-2-yl)phenylamino)-6-((1R,2S)-2-aminocyclohexylamino)pyridine-3,5-dicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 0.17 h

2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 1 h / 75 °C

3.1: potassium carbonate; dihydrogen peroxide / water; dimethyl sulfoxide / 0.08 h / 20 °C

With dihydrogen peroxide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;