Technology Process of 2,3-dicyano-6,7-di(4-tert-butyl)phenoxylnaphthalene
There total 2 articles about 2,3-dicyano-6,7-di(4-tert-butyl)phenoxylnaphthalene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: iodine / Cooling with ice
1.2: 20 h / -5 - 0 °C
2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 15 h / 95 °C / UV-irradiation
3.1: sodium iodide / N,N-dimethyl-formamide / 13 h / 80 °C / Inert atmosphere
4.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); iodine; potassium carbonate; sodium iodide;
In
tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2014.05.020
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 15 h / 95 °C / UV-irradiation
2: sodium iodide / N,N-dimethyl-formamide / 13 h / 80 °C / Inert atmosphere
3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; sodium iodide;
In
tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2014.05.020
- Guidance literature:
-
2,3-dicyano-6,7-di(4-tert-butyl)phenoxylnaphthalene;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
pentan-1-ol;
at 100 ℃;
for 1h;
Inert atmosphere;
gallium(III) trichloride;
In
pentan-1-ol;
for 37h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.dyepig.2014.05.020
