C₂₂H₃₀O₅

Base Information

Chemical Name:C₂₂H₃₀O₅
CAS No.:1440544-67-1
Molecular Formula:C₂₂H₃₀O₅
Molecular Weight:374.477
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>5</sub>

Synonyms:C₂₂H₃₀O₅

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Chemical Property of C₂₂H₃₀O₅

Chemical Property:

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Technology Process of C₂₂H₃₀O₅

There total 12 articles about C₂₂H₃₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: C₃₀H₃₈O₅

: 1440544-67-1
C₂₂H₃₀O₅

Guidance literature:: C₃₀H₃₈O₅; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; p-benzoquinone; In toluene; at 100 ℃; for 15h; Inert atmosphere;

In toluene; at 20 ℃;
DOI:10.1002/anie.201210266

Reference yield:

: 2-(4,6-di-O-(4-methoxybenzylidene)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl)-1-phenylethanone

: 1440544-67-1
C₂₂H₃₀O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogen / ethanol; ethyl acetate / 4 h

2.1: 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / toluene / 2.5 h / -15 - 20 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

5.1: dimethyl sulfoxide / 6 h / 50 °C / Inert atmosphere

6.1: potassium hydroxide; water / ethanol / Reflux

7.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

8.1: dmap / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

9.1: p-benzoquinone; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 15 h / 100 °C / Inert atmosphere

9.2: 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; water; hydrogen; diisobutylaluminium hydride; triethylamine; p-benzoquinone; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene;
DOI:10.1002/anie.201210266

Reference yield:

: 3-O-(3-oxo-phenylpropanoyl)-4,6-di-O-(4-methoxybenzylidene)-D-glucal

: 1440544-67-1
C₂₂H₃₀O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: palladium diacetate; 1,1'-bis-(diphenylphosphino)ferrocene / toluene / 2 h / 60 °C / Inert atmosphere; Schlenk technique

2.1: hydrogen / ethanol; ethyl acetate / 4 h

3.1: 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / toluene / 2.5 h / -15 - 20 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

6.1: dimethyl sulfoxide / 6 h / 50 °C / Inert atmosphere

7.1: potassium hydroxide; water / ethanol / Reflux

8.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

9.1: dmap / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

10.1: p-benzoquinone; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 15 h / 100 °C / Inert atmosphere

10.2: 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; 1,1'-bis-(diphenylphosphino)ferrocene; 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; water; hydrogen; palladium diacetate; diisobutylaluminium hydride; triethylamine; p-benzoquinone; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene;
DOI:10.1002/anie.201210266