C₅₅H₅₃N₅O₆SSi

Base Information

Chemical Name:C₅₅H₅₃N₅O₆SSi
CAS No.:1092804-03-9
Molecular Formula:C₅₅H₅₃N₅O₆SSi
Molecular Weight:940.207
Hs Code.:

C<sub>55</sub>H<sub>53</sub>N<sub>5</sub>O<sub>6</sub>SSi

Synonyms:C₅₅H₅₃N₅O₆SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₅H₅₃N₅O₆SSi

Chemical Property:

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Technology Process of C₅₅H₅₃N₅O₆SSi

There total 8 articles about C₅₅H₅₃N₅O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 956485-07-7
((3aR,6S,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxole-5,5-diyl)dimethanol

: 1092804-03-9
C₅₅H₅₃N₅O₆SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

3.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

3.2: 16.33 h / -78 - 20 °C

4.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

4.2: 4 h / 50 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.2: 0.5 h

6.1: n-butyllithium / tetrahydrofuran; hexanes / 2 h / 0 °C

6.2: 16 h / -78 - 20 °C

7.1: acetic anhydride; sulfuric acid; acetic acid

7.2: Reflux

8.1: dmap

With dmap; n-butyllithium; oxalyl dichloride; sulfuric acid; acetic anhydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; methanol; hexanes; dichloromethane; 7.2: Vorbrugen Reaction;

Reference yield:

: 956485-08-8
((3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 1092804-03-9
C₅₅H₅₃N₅O₆SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

2.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

2.2: 16.33 h / -78 - 20 °C

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

3.2: 4 h / 50 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

4.2: 0.5 h

5.1: n-butyllithium / tetrahydrofuran; hexanes / 2 h / 0 °C

5.2: 16 h / -78 - 20 °C

6.1: acetic anhydride; sulfuric acid; acetic acid

6.2: Reflux

7.1: dmap

With dmap; n-butyllithium; oxalyl dichloride; sulfuric acid; acetic anhydride; acetic acid; dimethyl sulfoxide; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; hexanes; dichloromethane; 6.2: Vorbrugen Reaction;

Reference yield:

: 939-26-4
2-bromomethylnaphthyl bromide

: 1092804-03-9
C₅₅H₅₃N₅O₆SSi

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1.17 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

7.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

7.2: 16.33 h / -78 - 20 °C

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

8.2: 4 h / 50 °C

9.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

9.2: 0.5 h

10.1: n-butyllithium / tetrahydrofuran; hexanes / 2 h / 0 °C

10.2: 16 h / -78 - 20 °C

11.1: acetic anhydride; sulfuric acid; acetic acid

11.2: Reflux

12.1: dmap

With dmap; sodium periodate; n-butyllithium; oxalyl dichloride; sulfuric acid; water; acetic anhydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; 11.2: Vorbrugen Reaction;