2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene

Base Information

Chemical Name:2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene
CAS No.:1437768-27-8
Molecular Formula:C₆₀H₃₀F₁₈I₃N₃
Molecular Weight:1515.6
Hs Code.:

Synonyms:2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene

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Chemical Property of 2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene

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Technology Process of 2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene

There total 1 articles about 2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 949529-68-4
3,4-bis(4-trifluoromethylphenyl)-1H-pyrrole

: 84322-56-5
1,3,5-trifluoro-2,4,6-triiodobenzene

: 1437768-27-8
2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene

Guidance literature:: 3,4-bis(4-trifluoromethylphenyl)-1H-pyrrole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.333333h; Inert atmosphere;

1,3,5-trifluoro-2,4,6-triiodobenzene; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja402371f

Reference yield: 69.0%

: 1437768-27-8
2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene

: 1416794-26-7
3,5-bisdodecyloxyphenylboronic acid

: C₁₅₀H₁₈₉F₁₈N₃O₆

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336; potassium carbonate; In water; toluene; Inert atmosphere; Reflux;
DOI:10.1021/ja402371f

Reference yield: 33.0%

: 3,5-bisbutoxyphenylboronic acid

: 1437768-27-8
2,4,6-tris[3,4-bis(4-trifluoromethylphenyl)-1H-pyrrolo]-1,3,5-triiodobenzene

: C₁₀₂H₉₃F₁₈N₃O₆

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336; potassium carbonate; In water; toluene; Inert atmosphere; Reflux;
DOI:10.1021/ja402371f