isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate

Base Information

Chemical Name:isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate
CAS No.:1427406-75-4
Molecular Formula:C₁₉H₂₀BrF₂NO₃
Molecular Weight:428.274
Hs Code.:

Synonyms:isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate

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Chemical Property of isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate

Chemical Property:

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Technology Process of isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate

There total 4 articles about isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 1427406-74-3
isopropyl 2-(3-amino-2,4-difluoro-phenoxy)acetate

: 51719-69-8
1-bromo-3-(bromomethyl)-5-methylbenzene

: 1427406-75-4
isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 100 ℃; for 1h; Microwave irradiation;

Reference yield:

: 1427330-97-9
3-amino-2 ,4-difluoro-phenol

: 1427406-75-4
isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / N,N-dimethyl-formamide / 0.58 h / 20 °C

2: potassium carbonate / dimethyl sulfoxide / 1 h / 100 °C / Microwave irradiation

With sodium carbonate; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 29921-57-1
isopropyl 2-bromoacetate

: 1427406-75-4
isopropyl 2-[3-[(3-bromo-5-methyl-phenyl)methylamino]-2,4-difluorophenoxy]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / N,N-dimethyl-formamide / 0.58 h / 20 °C

2: potassium carbonate / dimethyl sulfoxide / 1 h / 100 °C / Microwave irradiation

With sodium carbonate; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;