thiophosphoric acid S-(1,1-dimethyl-2-oxo-2-phenylethyl) ester O,O-diethyl ester

Base Information

Chemical Name:thiophosphoric acid S-(1,1-dimethyl-2-oxo-2-phenylethyl) ester O,O-diethyl ester
CAS No.:327619-21-6
Molecular Formula:C₁₄H₂₁O₄PS
Molecular Weight:316.358
Hs Code.:

Synonyms:thiophosphoric acid S-(1,1-dimethyl-2-oxo-2-phenylethyl) ester O,O-diethyl ester

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Chemical Property of thiophosphoric acid S-(1,1-dimethyl-2-oxo-2-phenylethyl) ester O,O-diethyl ester

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Technology Process of thiophosphoric acid S-(1,1-dimethyl-2-oxo-2-phenylethyl) ester O,O-diethyl ester

There total 2 articles about thiophosphoric acid S-(1,1-dimethyl-2-oxo-2-phenylethyl) ester O,O-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126-68-1
O,O,O-triethyl phosphorothioate

: 39158-85-5
2-methyl-1-phenyl-1-trimethylsiloxy-1-propene

: 327619-21-6
thiophosphoric acid S-(1,1-dimethyl-2-oxo-2-phenylethyl) ester O,O-diethyl ester

Guidance literature:: O,O,O-triethyl phosphorothioate; With sulfuryl dichloride; In dichloromethane; at 20 ℃; for 1h;

2-methyl-1-phenyl-1-trimethylsiloxy-1-propene; In dichloromethane; at -78 - 20 ℃;
DOI:10.1016/S0040-4020(03)00977-3

Reference yield:

: 611-70-1
phenyl isopropyl ketone

: 327619-21-6
thiophosphoric acid S-(1,1-dimethyl-2-oxo-2-phenylethyl) ester O,O-diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaI; Et₃N / acetonitrile / 60 °C

2.1: SO₂Cl₂ / CH₂Cl₂ / 1 h / 20 °C

2.2: 8.35 g / CH₂Cl₂ / -78 - 20 °C

With sulfuryl dichloride; triethylamine; sodium iodide; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(03)00977-3