Technology Process of C24H26O4
There total 5 articles about C24H26O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-hydroxy-5-methoxy-7-methylnaphthalen-1-yl pivalate;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.166667h;
Inert atmosphere;
benzyl bromide;
In
N,N-dimethyl-formamide;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ja409669r
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
1.2: 0.5 h / -78 °C
2.1: dichloromethane / 20 h / 20 °C
2.2: 0.5 h / 20 °C
3.1: sodium dithionite dihydrate / dichloromethane; water / 1 h / 20 °C / Inert atmosphere
4.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere
5.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere
5.2: 20 °C / Inert atmosphere
With
sodium dithionite dihydrate; sodium hydride; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
2.1: |Diels-Alder Cycloaddition / 2.2: |Diels-Alder Cycloaddition;
DOI:10.1021/ja409669r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium dithionite dihydrate / dichloromethane; water / 1 h / 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere
3.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
sodium dithionite dihydrate; sodium hydride; triethylamine;
In
dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja409669r
