C₆₁H₈₅NO₁₂Si

Base Information

Chemical Name:C₆₁H₈₅NO₁₂Si
CAS No.:1448230-76-9
Molecular Formula:C₆₁H₈₅NO₁₂Si
Molecular Weight:1052.43
Hs Code.:

C<sub>61</sub>H<sub>85</sub>NO<sub>12</sub>Si

Synonyms:C₆₁H₈₅NO₁₂Si

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Chemical Property of C₆₁H₈₅NO₁₂Si

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Technology Process of C₆₁H₈₅NO₁₂Si

There total 15 articles about C₆₁H₈₅NO₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 994-30-9
triethylsilyl chloride

: 1448230-75-8
C₅₅H₇₁NO₁₂

: 1448230-76-9
C₆₁H₈₅NO₁₂Si

Guidance literature:: With pyridine; silver nitrate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-65-6
C₃₂H₆₇IO₄Si₂

: 1448230-76-9
C₆₁H₈₅NO₁₂Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

1.2: 0.33 h / 20 °C

1.3: 13 h / 50 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

3.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

4.1: acetic acid / tetrahydrofuran; water / 16 h / 20 °C

5.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

6.2: 12 h / 0 - 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; hexane / 2.25 h / -78 °C

8.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C

9.1: triethylamine; di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C

9.2: 2.25 h / -78 - 0 °C

9.3: 1 h / 0 °C

10.1: pyridine; silver nitrate / N,N-dimethyl-formamide / 1 h / 20 °C

With pyridine; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tert.-butyl lithium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; silver nitrate; acetic acid; triethylamine; 9-methoxy-9-BBN; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; pentane; 9.1: |Evans Aldol Reaction / 9.2: |Evans Aldol Reaction;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-61-2
C₂₂H₃₆O₆

: 1448230-76-9
C₆₁H₈₅NO₁₂Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.17 h / 20 °C / pH 7

3.1: triethylamine; dmap / dichloromethane / 25 h / 0 - 20 °C

4.1: sodium iodide / acetone / 18 h / 50 °C

5.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

5.2: 0.33 h / 20 °C

5.3: 13 h / 50 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

7.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

8.1: acetic acid / tetrahydrofuran; water / 16 h / 20 °C

9.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

10.2: 12 h / 0 - 20 °C

11.1: diisobutylaluminium hydride / dichloromethane; hexane / 2.25 h / -78 °C

12.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C

13.1: triethylamine; di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C

13.2: 2.25 h / -78 - 0 °C

13.3: 1 h / 0 °C

14.1: pyridine; silver nitrate / N,N-dimethyl-formamide / 1 h / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tert.-butyl lithium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; silver nitrate; acetic acid; triethylamine; 9-methoxy-9-BBN; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; mineral oil; pentane; 13.1: |Evans Aldol Reaction / 13.2: |Evans Aldol Reaction;
DOI:10.1021/ol4017518