Technology Process of C16H18ClNO7
There total 9 articles about C16H18ClNO7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride; N,N-dimethyl-formamide;
In
dichloromethane;
at 20 ℃;
Cooling with ice;
Inert atmosphere;
DOI:10.1002/pola.25845
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere
1.2: 2 h / 20 °C
2.1: phosphorus pentachloride / 0.5 h / 20 °C / Inert atmosphere
With
phosphorus pentachloride; triethylamine;
In
tetrahydrofuran;
DOI:10.1021/ma9023679
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 25 °C
2: nitric acid; acetic anhydride / 3 h / 0 °C
3: methanol; sodium tetrahydroborate / tetrahydrofuran / 16 h / 25 °C
4: water; sodium hydroxide / 7 h / 25 °C
5: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
6: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C / Cooling with ice; Inert atmosphere
With
methanol; sodium tetrahydroborate; oxalyl dichloride; water; nitric acid; acetic anhydride; potassium carbonate; triethylamine; N,N-dimethyl-formamide; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/pola.25845
