methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate

Base Information

• Chemical Name: methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate
• CAS No.: 130145-36-7
• Molecular Formula: C₂₀H₂₄N₄O₈
• Molecular Weight: 448.433

Synonyms:methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate

Chemical Property of methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate

Chemical Property:

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Technology Process of methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate

There total 2 articles about methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2-amino-2-phenylacetaldehyde diethyl acetal (67601-99-4) + methyl (4-chloro-3,5-dinitrophenyl)carbamate (130145-34-5) → methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate (130145-36-7)

Guidance literature:

With triethylamine; In ethanol; for 18h; Heating;

DOI:10.1021/jm00173a021

Reference yield:

2-Chloro-5-isocyanato-1,3-dinitro-benzene (467443-76-1) → methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate (130145-36-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 18 h / Ambient temperature

2: 81 percent / Et₃N / ethanol / 18 h / Heating

With triethylamine; In ethanol;

DOI:10.1021/jm00173a021

Reference yield:

methyl <4-<(2,2-diethoxy-1-phenylethyl)amino>-3,5-dinitrophenyl>carbamate (130145-36-7) → [3,5-Diamino-4-(2,2-diethoxy-1-phenyl-ethylamino)-phenyl]-carbamic acid methyl ester

Guidance literature:

With hydrogen; nickel; In ethanol; for 4h;

DOI:10.1021/jm00173a021

upstream raw materials:

2-amino-2-phenylacetaldehyde diethyl acetal

methyl (4-chloro-3,5-dinitrophenyl)carbamate

2-Chloro-5-isocyanato-1,3-dinitro-benzene

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