N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide

Base Information

• Chemical Name: N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide
• CAS No.: 935981-26-3
• Molecular Formula: C₆₁H₅₈BrN₃O₇
• Molecular Weight: 1025.05
• Mol file: 935981-26-3.mol

Synonyms:N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide

Chemical Property of N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide

There total 1 articles about N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

N-t-butoxycarbonyl-tyramine (64318-28-1) + 1,7-dibromo-N,N'-bis(2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic acid diimide (331861-94-0) → N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide (935981-26-3)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In toluene; for 2h; Heating;

DOI:10.1021/jo0624748

Reference yield: 98.0%

N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide (935981-26-3) + phenylboronic acid (98-80-6) → C67H63N3O7

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; at 80 ℃; for 3h;

DOI:10.1021/jo0624748

Reference yield: 78.0%

N,N'-di-(2,6-diisopropylphenyl)-1,7-dibromoperylene-3,4,9,10-tetracarboxylic acid diimide (935981-26-3) → C61H59N3O8

Guidance literature:

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 100 ℃; for 10h;

DOI:10.1021/jo0624748

upstream raw materials:

N-t-butoxycarbonyl-tyramine

1,7-dibromo-N,N'-bis(2,6-diisopropylphenyl)perylene-3,4:9,10-tetracarboxylic acid diimide