3-Bromo-2-iodobenzonitrile

Base Information

Chemical Name:3-Bromo-2-iodobenzonitrile
CAS No.:450412-21-2
Molecular Formula:C₇H₃BrIN
Molecular Weight:307.916
Hs Code.:
European Community (EC) Number:877-609-0
Nikkaji Number:J1.780.438C

Synonyms:3-bromo-2-iodobenzonitrile;450412-21-2;2-Iodo-3-bromobenzonitrile;SCHEMBL9407871;MFCD18391644;AKOS033573777;CS-0191214;E91503;EN300-141007;Z1269146738

Suppliers and Price of 3-Bromo-2-iodobenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-Bromo-2-iodobenzonitrile

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:306.84936
Heavy Atom Count:10
Complexity:162

Purity/Quality:: 99% HPLC ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Br)I)C#N

Technology Process of 3-Bromo-2-iodobenzonitrile

There total 1 articles about 3-Bromo-2-iodobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 6952-59-6
3-cyanobromobenzene

: 450412-21-2
1-bromo-2-cyano-3-iodobenzene

Guidance literature:: 3-cyanobromobenzene; With tBu₂Zn(TMP)Li; In tetrahydrofuran; at 0 ℃; for 3.5h;

With iodine; In tetrahydrofuran; at 20 ℃; for 12h; Further stages.;
DOI:10.1021/ja0202199

Reference yield: 76.0%

: 73183-34-3
bis(pinacol)diborane

: 450412-21-2
1-bromo-2-cyano-3-iodobenzene

: 214360-46-0
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile

Guidance literature:: bis(pinacol)diborane; With dimethyl zinc(II); magnesium 2-methylpropan-2-olate; In 1,4-dioxane; hexane; at 0 - 20 ℃; for 0.5h; Schlenk technique; Glovebox; Inert atmosphere;

1-bromo-2-cyano-3-iodobenzene; In 1,4-dioxane; hexane; at 20 - 120 ℃; for 24h; Schlenk technique; Glovebox; Inert atmosphere;

With water; In 1,4-dioxane; hexane; at 20 ℃; for 0.0833333h; regioselective reaction; Schlenk technique; Glovebox; Inert atmosphere;
DOI:10.1021/ja409748m

Reference yield: 60.0%

: 153782-96-8
(S)-N-t-butoxycarbonyl-2-phenylmethyl aziridine

: 450412-21-2
1-bromo-2-cyano-3-iodobenzene

: 1142923-84-9
C₂₁H₂₃BrN₂O₂

Guidance literature:: 1-bromo-2-cyano-3-iodobenzene; With n-butyllithium; In hexane; toluene; at -78 ℃;

(S)-N-t-butoxycarbonyl-2-phenylmethyl aziridine; With boron trifluoride diethyl etherate; In toluene; at -78 ℃;
DOI:10.1016/j.tetlet.2009.02.047