N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide

Base Information

Chemical Name:N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide
CAS No.:668988-28-1
Molecular Formula:C₂₇H₂₆N₂O₄
Molecular Weight:442.514
Hs Code.:

Synonyms:N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide

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Chemical Property of N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide

Chemical Property:

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Technology Process of N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide

There total 4 articles about N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 668988-21-4
N-((1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)-1-phenylmethyl)-N-benzylbenzamide

: 668988-28-1
N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide

Guidance literature:: With 4 A molecular sieve; potassium tert-butylate; In tetrahydrofuran; tert-butyl alcohol; at 0 ℃; for 0.166667h;
DOI:10.1055/s-2003-43355

Reference yield:

: 30093-99-3
4,4-dimethyl-2-oxazoline

: 668988-28-1
N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 49.7 percent / tetrahydrofuran; hexane / -78 - 20 °C

2.1: 88 percent / methanol / 1 h / 20 °C

3.1: 89 percent / 4 Angstroem molecular sieves; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.17 h / 0 °C

With n-butyllithium; 4 A molecular sieve; potassium tert-butylate; In tetrahydrofuran; methanol; hexane; tert-butyl alcohol; 2.1: Ugi four-component condensation;
DOI:10.1055/s-2003-43355

Reference yield:

: 100-52-7
benzaldehyde

: 668988-28-1
N-((4,4-dimethyl-2-oxo-3-oxazolidinyl)carbonyl-1-phenylmethyl)-N-benzylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / methanol / 1 h / 20 °C

2: 89 percent / 4 Angstroem molecular sieves; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.17 h / 0 °C

With 4 A molecular sieve; potassium tert-butylate; In tetrahydrofuran; methanol; tert-butyl alcohol; 1: Ugi four-component condensation;
DOI:10.1055/s-2003-43355