1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane

Base Information

Chemical Name:1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane
CAS No.:1073314-31-4
Molecular Formula:C₃₅H₆₁N₅O₆
Molecular Weight:647.899
Hs Code.:

Synonyms:1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane

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Chemical Property of 1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane

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Technology Process of 1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane

There total 1 articles about 1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 878779-86-3
1,4,7-tri-tert-butyl 10-(3-(bromomethyl)benzyl)-1,4,7,10-tetraazacyclododecane-1,4,7-tricarboxylate

: 109-89-7
diethylamine

: 1073314-31-4
1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane

Guidance literature:: In acetonitrile; at 20 ℃; for 6h;
DOI:10.1021/ja8037799

Reference yield:

: 1073314-31-4
1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane

: 1073314-32-5
1-[3'-(N,N-diethylaminomethyl)benzyl]-1,4,7,10-tetraazacyclododecane

Guidance literature:: 1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecane; With hydrogenchloride; In ethanol; water; at 20 ℃; for 8h;

In water; pH=12.5; Alkaline conditions;
DOI:10.1021/ja8037799