3-(3,5-dimethoxyphenyl)-N²,N²-bis(4-methoxybenzyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine

Base Information

• Chemical Name: 3-(3,5-dimethoxyphenyl)-N²,N²-bis(4-methoxybenzyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine
• CAS No.: 311820-03-8
• Molecular Formula: C₅₁H₄₆N₄O₄
• Molecular Weight: 778.951

Synonyms:3-(3,5-dimethoxyphenyl)-N²,N²-bis(4-methoxybenzyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine

Chemical Property of 3-(3,5-dimethoxyphenyl)-N²,N²-bis(4-methoxybenzyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3-(3,5-dimethoxyphenyl)-N²,N²-bis(4-methoxybenzyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine

There total 4 articles about 3-(3,5-dimethoxyphenyl)-N²,N²-bis(4-methoxybenzyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methoxybenzyl chloride (824-94-2) + 3-(3,5-dimethoxyphenyl)-N7-trityl-1,6-naphthyridine-2,7-diamine (311820-00-5) → 3-(3,5-dimethoxyphenyl)-N2,N2-bis(4-methoxybenzyl)-N7-trityl-1,6-naphthyridine-2,7-diamine (311820-03-8)

Guidance literature:

3-(3,5-dimethoxyphenyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.0333333h;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Further stages.;

DOI:10.1021/jm000161d

Reference yield:

trityl chloride (76-83-5) → 3-(3,5-dimethoxyphenyl)-N2,N2-bis(4-methoxybenzyl)-N7-trityl-1,6-naphthyridine-2,7-diamine (311820-03-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.42 h / 20 °C

1.2: 40 percent / 24 h / 20 °C

2.1: NaH / dimethylformamide / 0.03 h / 20 °C

2.2: dimethylformamide / 2 h / 20 °C

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1021/jm000161d

Reference yield:

3-(3,5-Dimethoxyphenyl)-1,6-naphthyridine-2,7-diamine (293301-09-4) → 3-(3,5-dimethoxyphenyl)-N2,N2-bis(4-methoxybenzyl)-N7-trityl-1,6-naphthyridine-2,7-diamine (311820-03-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.42 h / 20 °C

1.2: 40 percent / 24 h / 20 °C

2.1: NaH / dimethylformamide / 0.03 h / 20 °C

2.2: dimethylformamide / 2 h / 20 °C

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1021/jm000161d

upstream raw materials:

p-methoxybenzyl chloride

3-(3,5-dimethoxyphenyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine

trityl chloride

3-(3,5-Dimethoxyphenyl)-1,6-naphthyridine-2,7-diamine

Downstream raw materials:

3-(3,5-dimethoxyphenyl)-N²,N²,N⁷,N⁷-tetrakis(4-methoxybenzyl)-1,6-naphthyridine-2,7-diamine

3-(3,5-dimethoxyphenyl)-N⁷-trityl-1,6-naphthyridine-2,7-diamine

N-[2-[[(tert-butylamino)carbonyl]amino]-3-(3,5-dimethoxyphenyl)-1,6-naphthyridin-7-yl]acetamide

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