Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine

Base Information

Chemical Name:Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine
CAS No.:159421-31-5
Molecular Formula:C₂₂H₃₁NSi₂
Molecular Weight:365.666
Hs Code.:

Synonyms:Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine

Suppliers and Price of Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine

Chemical Property:

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Technology Process of Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine

There total 5 articles about Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 159421-29-1
N--2-butynylamine

: 159421-31-5
Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine

Guidance literature:: With potassium carbonate; In acetonitrile; at 23 ℃;
DOI:10.1021/jo00100a003

Reference yield:

: 2975-46-4
3-(trimethylsilyl)prop-2-yn-1-al

: 159421-31-5
Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 987 mg / MgSO₄ / benzene / 1 h / Ambient temperature

2: 1.) BF₃*Et₂O / 1.) THF, hexane, -78 deg C, 10 min; 2.) THF, -78 deg C, 10 min

3: K₂CO₃ / acetonitrile / 16 h / Ambient temperature

With boron trifluoride diethyl etherate; magnesium sulfate; potassium carbonate; In acetonitrile; benzene;
DOI:10.3987/com-96-s43

Reference yield:

: 54655-07-1
lithium trimethylsilylacetylenide

: 159421-31-5
Benzyl-but-3-ynyl-(3-trimethylsilanyl-1-trimethylsilanylethynyl-prop-2-ynyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BF₃*Et₂O / 1.) THF, hexane, -78 deg C, 10 min; 2.) THF, -78 deg C, 10 min

2: K₂CO₃ / acetonitrile / 16 h / Ambient temperature

With boron trifluoride diethyl etherate; potassium carbonate; In acetonitrile;
DOI:10.3987/com-96-s43