(2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone

Base Information

Chemical Name:(2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone
CAS No.:131288-31-8
Molecular Formula:C₂₇H₂₅NO₄
Molecular Weight:427.5
Hs Code.:

Synonyms:(2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone

Chemical Property:

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Technology Process of (2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone

There total 1 articles about (2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 556-56-9
allyl iodid

: 95260-60-9
(2S,4S)-benzyl 4-benzyl-5-oxo-2-phenyloxazolidine-3-carboxylate

: 131288-31-8
(2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone

Guidance literature:: With potassium hexamethylsilazane; Yield given; Multistep reaction; 1.) THF, toluene, 30 min, 2.) THF, toluene, a) -78 deg C, 3 h, b) from -78 deg C to RT, 4 h;
DOI:10.1021/jm990140n

Reference yield: 100.0%

: 131288-31-8
(2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone

: 131288-65-8
(2S)-N-(benzyloxycarbonyl)-2-allylphenylalanine

Guidance literature:: With sodium hydroxide; In methanol; for 16h; Heating;
DOI:10.1021/jm990140n

Reference yield:

: 131288-31-8
(2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone

: 239437-74-2
(2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 1 N aq.NAOH / methanol / 16 h / Heating

2: OsO₄, NaIO₄ / tetrahydrofuran; ethyl acetate / 24 h

With sodium hydroxide; sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1021/jm990140n