2-azetidinepropanamide, N-<(4-methylphenyl)sulfonyl>-1-(phenylmethoxy)-4-oxo

Base Information

Chemical Name:2-azetidinepropanamide, N-<(4-methylphenyl)sulfonyl>-1-(phenylmethoxy)-4-oxo
CAS No.:157732-79-1
Molecular Formula:C₂₀H₂₂N₂O₅S
Molecular Weight:402.471
Hs Code.:

Synonyms:2-azetidinepropanamide, N-<(4-methylphenyl)sulfonyl>-1-(phenylmethoxy)-4-oxo

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Chemical Property of 2-azetidinepropanamide, N-<(4-methylphenyl)sulfonyl>-1-(phenylmethoxy)-4-oxo

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Technology Process of 2-azetidinepropanamide, N-<(4-methylphenyl)sulfonyl>-1-(phenylmethoxy)-4-oxo

There total 2 articles about 2-azetidinepropanamide, N-<(4-methylphenyl)sulfonyl>-1-(phenylmethoxy)-4-oxo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 70-55-3
toluene-4-sulfonamide

: 157732-53-1
2-azetidinepropanoic acid, 1-(phenylmethoxy)-4-oxo

: 157732-79-1
2-azetidinepropanamide, N-<(4-methylphenyl)sulfonyl>-1-(phenylmethoxy)-4-oxo

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85552-6

Reference yield:

: 157435-83-1
(R)-2-Azetidinepropanoic acid 4-oxo-1-(phenylmethoxy)-(1,1-dimethylethyl) ester

: 157732-79-1
2-azetidinepropanamide, N-<(4-methylphenyl)sulfonyl>-1-(phenylmethoxy)-4-oxo

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / anisole, trifluoroacetic acid / CH₂Cl₂ / 2.5 h / 0 °C

2: 85 percent / dimethylaminopyridine, 1-ethyl-3-(dimethylaminopropyl)carbodiimide*HCl / CH₂Cl₂ / 48 h / Ambient temperature

With dmap; methoxybenzene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)85552-6