C₂₁H₂₁N₄PS₃

Base Information

• Chemical Name: C₂₁H₂₁N₄PS₃
• CAS No.: 1260152-38-2
• Molecular Formula: C₂₁H₂₁N₄PS₃
• Molecular Weight: 456.596
• Mol file: 1260152-38-2.mol

Synonyms:C₂₁H₂₁N₄PS₃

Chemical Property of C₂₁H₂₁N₄PS₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₂₁N₄PS₃

There total 5 articles about C₂₁H₂₁N₄PS₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

C20H19N4PS3 (1260152-21-3) + methyl iodide (74-88-4) → C21H21N4PS3 (1260152-38-2)

Guidance literature:

With sodium ethanolate; In ethanol; at 20 ℃; for 12h;

DOI:10.1002/hc.20638

Reference yield:

C13H14N4O (1260152-03-1) → C21H21N4PS3 (1260152-38-2)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine; hydrogen sulfide; triethylamine / 20 °C

2: pyridine; tetraphosphorus decasulfide / 4 h / Reflux

3: sodium ethanolate / ethanol / 0.02 h / Reflux

4: sodium ethanolate / ethanol / 12 h / 20 °C

With pyridine; tetraphosphorus decasulfide; hydrogen sulfide; sodium ethanolate; triethylamine; In ethanol;

DOI:10.1002/hc.20638

Reference yield:

N-(2,2-dichloro-1-cyanovinyl)-4-methylbenzamide (61767-26-8) → C21H21N4PS3 (1260152-38-2)

Guidance literature:

Multi-step reaction with 5 steps

1: isopropyl alcohol / 0.08 h / 20 °C

2: pyridine; hydrogen sulfide; triethylamine / 20 °C

3: pyridine; tetraphosphorus decasulfide / 4 h / Reflux

4: sodium ethanolate / ethanol / 0.02 h / Reflux

5: sodium ethanolate / ethanol / 12 h / 20 °C

With pyridine; tetraphosphorus decasulfide; hydrogen sulfide; sodium ethanolate; triethylamine; In ethanol; isopropyl alcohol;

DOI:10.1002/hc.20638

upstream raw materials:

C₁₃H₁₆N₄OS

C₂₀H₁₉N₄PS₃

methyl iodide

C₁₃H₁₄N₄O