Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

Base Information

Chemical Name:Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate
CAS No.:112888-79-6
Molecular Formula:C₂₉H₃₂N₄O₆S
Molecular Weight:564.662
Hs Code.:

Diethyl N-<4-<N-<<3,4-dihydro-2-(methylthio)-4-oxo-6-quinazolinyl>methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

Synonyms:Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

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Chemical Property of Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

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Technology Process of Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

There total 5 articles about Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 118111-63-0
Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

: 74-88-4
methyl iodide

: 112888-79-6
Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

Guidance literature:: With ammonium hydroxide; In ethanol; water; for 1h; Ambient temperature;
DOI:10.1021/jm00123a010

Reference yield:

: 76858-72-5
diethyl N-(4-(prop-2-ynylamino)benzoyl)-L-glutamate

: 112888-79-6
Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / CaCO₃ / dimethylformamide / 16 h / 60 °C

2: 45 percent / thiourea, formic acid / ethanol / 0.25 h / Heating

3: 81 percent / aq. NH₃ / H₂O; ethanol / 1 h / Ambient temperature

With ammonium hydroxide; formic acid; thiourea; calcium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00123a010

Reference yield:

: 118111-59-4
6-Bromomethyl-2-chloro-3H-quinazolin-4-one

: 112888-79-6
Diethyl N-<4-methyl>-N-prop-2-ynylamino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / CaCO₃ / dimethylformamide / 16 h / 60 °C

2: 45 percent / thiourea, formic acid / ethanol / 0.25 h / Heating

3: 81 percent / aq. NH₃ / H₂O; ethanol / 1 h / Ambient temperature

With ammonium hydroxide; formic acid; thiourea; calcium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00123a010