N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine

Base Information

Chemical Name:N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine
CAS No.:809277-31-4
Molecular Formula:C₁₆H₂₉BN₆O₂
Molecular Weight:348.256
Hs Code.:

Synonyms:N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine

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Chemical Property of N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine

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Technology Process of N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine

There total 3 articles about N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(4,5-dihydro-1H-imidazol-2-yl)-nitrilo-2,2',2''-triethanamine hydrochloride

: 40138-16-7
2-formylbenzene boronic acid

: 809277-31-4
N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine

: C₂₃H₃₆B₂N₆O₄

Guidance literature:: N-(4,5-dihydro-1H-imidazol-2-yl)-nitrilo-2,2',2''-triethanamine hydrochloride; 2-formylbenzene boronic acid; With triethylamine; In methanol; at 20 ℃; for 6h;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 12h; Title compound not separated from byproducts;
DOI:10.1002/chem.200400369

Reference yield:

: 809277-29-0
di-tert-butyl-N''-(4,5-dihydro-1H-imidazol-2-yl)-nitrilo-2,2',2''-triethanamine-N,N'-dicarboxylate

: 809277-31-4
N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 87 percent / aq. HCl / ethanol / 1.5 h / 20 °C

2.1: Et₃N / methanol / 6 h / 20 °C

2.2: NaBH₄ / methanol / 12 h / 20 °C

With hydrogenchloride; triethylamine; In methanol; ethanol;
DOI:10.1002/chem.200400369

Reference yield:

: 161038-11-5
{2-[(2-amino-ethyl)-(2-tert-butoxycarbonylamino-ethyl)-amino]-ethyl}-carbamic acid tert-butyl ester

: 809277-31-4
N-(4,5-dihydro-1H-imidazol-2-yl)-N'-(2-dihydroxyboranylphenyl)-nitrilo-2,2',2''-triethanamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 5 h / Heating

2.1: 87 percent / aq. HCl / ethanol / 1.5 h / 20 °C

3.1: Et₃N / methanol / 6 h / 20 °C

3.2: NaBH₄ / methanol / 12 h / 20 °C

With hydrogenchloride; triethylamine; In methanol; ethanol;
DOI:10.1002/chem.200400369