tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate

Base Information

Chemical Name:tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate
CAS No.:1364929-00-9
Molecular Formula:C₂₅H₂₄Cl₃F₃N₂O₃
Molecular Weight:563.831
Hs Code.:

Synonyms:tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Useful:

Technology Process of tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate

There total 4 articles about tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338926-69-4
tert-butyl {5-[4,4,4-trifluoro-3-(nitromethyl)-3-(3,4,5-trichlorophenyl)-butanoyl]-2,3-dihydro-1H-inden-1-yl}carbamate

: 1364929-00-9
tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate

Guidance literature:: With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In 1,4-dioxane; methanol; for 1h; Inert atmosphere; Cooling with ice;

Reference yield:

: 158401-00-4
1-(3,4,5-trichloro-phenyl)-2,2,2-trifluoro-ethanone

: 1364929-00-9
tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydride / tetrahydrofuran / 8 h / Reflux

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 10 h / 20 °C

3: sodium tetrahydroborate; nickel(II) chloride hexahydrate / 1,4-dioxane; methanol / 1 h / Inert atmosphere; Cooling with ice

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; lithium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;

Reference yield:

: 1338926-80-9
tert-butyl N-(5-acetylindan-1-yl)carbamate

: 1364929-00-9
tert-butyl {5-[1-oxide-3-(3,4,5-trichlorophenyl)-3-(trifluoromethyl)-3,4-dihydro-2H-pyrrol-5-yl]-2,3-dihydro-1H-inden-1-yl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydride / tetrahydrofuran / 8 h / Reflux

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 10 h / 20 °C

3: sodium tetrahydroborate; nickel(II) chloride hexahydrate / 1,4-dioxane; methanol / 1 h / Inert atmosphere; Cooling with ice

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; lithium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;